Agree with the above comment - I think it was NRFTW, concerning saying yes to using his demon powers, to Ruby.
Now he implied a similar thing about Adam saying Yes -- here's the passage and see if that's what is tripping your memory:
5.18 Point of No Return
Dean: I’m not letting him do it. Sam: Who, Adam? No, I'm... I'm not, either. Dean: No, you're not getting me. Sam: Oh, no, no, I "get" you perfectly. But I'm not letting you do it, either. Dean: That kid's not taking a bullet for me. Sam: Dean
( ... )
I think maybe you're thinking of the start of 5.20
Dean: What the hell is wrong with you? Sam: Dean - Dean: Don't Dean me, you have had some stupid ideas in the past, but this! Did you know about this? Bobby: What? Dean: About Sam's genius plan to say yes to the devil? Bobby: *nods* Dean: WELL THANKS FOR THE HEADS-UP! You can't do this. Sam: If that's the consensus. Dean: All right, awesome. End of discussion.
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Aw, I knew you'd show up. Because I knew SAM wouldn't listen.
SAM looks at him on that note but looks away quickly.
DEAN
But you're not gonna teach him anything, you understand me? Over my dead body.
RUBY
Oh. Well, you're right about that.
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Now he implied a similar thing about Adam saying Yes -- here's the passage and see if that's what is tripping your memory:
5.18 Point of No Return
Dean: I’m not letting him do it.
Sam: Who, Adam? No, I'm... I'm not, either.
Dean: No, you're not getting me.
Sam: Oh, no, no, I "get" you perfectly. But I'm not letting you do it, either.
Dean: That kid's not taking a bullet for me. Sam: Dean ( ... )
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Dean: What the hell is wrong with you?
Sam: Dean -
Dean: Don't Dean me, you have had some stupid ideas in the past, but this! Did you know about this?
Bobby: What?
Dean: About Sam's genius plan to say yes to the devil?
Bobby: *nods*
Dean: WELL THANKS FOR THE HEADS-UP! You can't do this.
Sam: If that's the consensus.
Dean: All right, awesome. End of discussion.
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